Publication details

OPTIMIZATION OF THE SEPARATION OF MICRON-SIZED LATEX-PARTICLES BY GRAVITATIONAL FIELD-FLOW FRACTIONATION

Authors

PAZOUREK Jiří CHMELIK J

Year of publication 1993
Type Peer-reviewed scientific article
Magazine / Source CHROMATOGRAPHIA
MU Faculty or unit

Faculty of Pharmacy

Citation
web https://link.springer.com/article/10.1007/BF02267922
Doi https://doi.org/10.1007/bf02267922
Keywords FIELD-FLOW FRACTIONATION; OPTIMIZATION; LATEX PARTICLES; LIFT FORCES
Description Optimization of separation of latex particles by gravitational field-flow fractionation is described. The separation was performed in a ribbon-like glass wall channel 36 cm long; the steps of optimization were performed on the basis of both theoretical considerations and experimental measurements. Theoretical considerations were based on separation governed by the Earth's gravity and lift forces. The experimental conditions optimized were the quality of the surface of the channel wall and the type and concentration of the carrier liquid surfactant. As a result of the optimization it was possible to separate 5, 7, 10, 15, and 20 mum diameter particles in 4 min, using a 0.01 % solution of Tween 60 (nonionic surfactant) in an 80 mum high channel with its bottom modified by MS200 silicon oil.

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