Publication details

On the design of a monolithic 4-bounce high resolution X-ray monochromator

Authors

VAGOVIČ P. KORYTÁR D. MIKULÍK Petr FERRARI C.

Year of publication 2007
Type Article in Periodical
Magazine / Source Nuclear Instruments and Methods in Physics Research Section B
MU Faculty or unit

Faculty of Science

Citation
Web http://www.sci.muni.cz/~mikulik/Publications.html#VagovicKorytarMikulikF-nimb-2007
Field Solid matter physics and magnetism
Keywords X-ray monochromator; High resolution; In-line optics; Spectral-angular function; Vertical dispersion
Description A monolithic monochromator (+n, -n, -m, +m) made of a single block of Ge crystal designed for CoKalpha1 radiation was developed and tested numerically and experimentally by means of X-ray diffraction. The advantage of monolithic devices is their mechanical stability and the alignment of such optics is much easier than with polylithic optics, but the development of these devices is rather demanding. The presented monochromator belongs to a group of coplanar in-line devices, which means that the input beam is parallel with the output beam. For the estimation of the spectral and angular properties of a diffracted beam of this monochromator (such as bandpass width, output divergence and input acceptance) we used a numerical approach which we call spectral-angular function. It takes into account both the vertical and the horizontal divergence of the input radiation and uses two-beam X-ray dynamical theory of diffraction. Experimentally, the monochromator was tested by means of X-ray diffraction (synchrotron radiation testing) and the results from this characterization are presented. The influence of the vertical divergence on the spectral distribution of the diffracted beam is discussed and compared with previously published analytical results.
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