Publication details
Vsázková technologie výroby 4,4-dimethyl-3-oxopentannitrilu
| Title in English | Manufacturing of 4,4-dimethyl-3-oxopentanenitrile |
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| Authors | |
| Year of publication | 2013 |
| MU Faculty or unit | |
| Description | Its a manufacturing process. Discontinual technology process is based on a susbstitution reaction of chlorine atom in 1-chloro-3,3-dimethylbutan-2-one by the action of cyanide anion in methanol solution. Formation of an undesirable oxirane by-product (20-35 %) is eliminated by an addition of a catalytic amount of iodide (Finkelstein catalytic route) and the target product is obtained in min. yield 95 % and purity min. 99 %. |
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