Publication details
Phenyl bis(morpholin-4-ylamido)phosphinate
| Authors | |
|---|---|
| Year of publication | 2011 |
| Type | Article in Periodical |
| Magazine / Source | Acta Crystallographica Section E: Structure Reports Online |
| MU Faculty or unit | |
| Citation | |
| Web | https://journals.iucr.org/e/issues/2011/08/00/gk2392/ |
| Doi | http://dx.doi.org/10.1107/S1600536811029734 |
| Keywords | single-crystal X-ray study; T = 120 K; mean (C–C) = 0.002 angstrom; disorder in main residue; R factor = 0.029; wR factor = 0.070; data-to-parameter ratio = 11.0 |
| Description | In the title compound, C14H23N4O4P, the P atom is in a distorted tetrahedral environment with bond angles in the range 96.87 (6)-119.86 (6)degrees. The two morpholinyl groups adopt a chair conformation. The phenyl ring is disordered over two sets of sites with equal occupancies [0.500 (2)]. In the crystal, adjacent molecules are linked via N-H center dot center dot center dot O hydrogen bonds into an extended chain running parallel to the a axis. Only one of the amidate N-H groups is involved in hydrogen bonding. |